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Researchers who escalated too quickly bore the brunt of gastrointestinal side effects, while those who followed the standard four-week titration intervals reported significantly better tolerability

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Samples were loaded onto a precolumn (Acclaim PepMap 100, C18, 75 m 2 cm, 3-m particle size) and separated with an Easy-Spray analytical column (PepMap RSLC, C18, 75 m 50 cm, 2 m particle size) at 40 C using a two-solvent system: (A) 0.1% formic acid in water, (B) 0.1% formic acid in acetonitrile

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